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Beilstein J. Org. Chem. 2015, 11, 85–91, doi:10.3762/bjoc.11.12
Graphical Abstract
Scheme 1: Anodic fluorination of sulfides having an electron-withdrawing group.
Scheme 2: Anodic fluorination of dithioacetals.
Figure 1: Dependency of fluorinated product selectivity on a series of fluoride salts (a) Et3N·nHF (n = 3–5) ...
Scheme 3: Plausible reaction mechanism for anodic fluorination of 1b, 1d, and 1f.
Scheme 4: Mechanism for suppression of the elimination of HF (deprotonation) and preferable desulfurization o...